JACoW is a publisher in Geneva, Switzerland that publishes the proceedings of accelerator conferences held around the world by an international collaboration of editors.
TY - CONF AU - Yang, Z.T. AU - Hao, J.K. AU - Liu, K.X. AU - Quan, S.W. ED - Saito, Kenji ED - Xu, Ting ED - Sakamoto, Naruhiko ED - Schaa, Volker R.W. ED - Thomas, Paul W. TI - The Oxidizing Responses of Baked Niobium Exposed to Various Gases via In-situ NAXPS J2 - Proc. of SRF2023, Grand Rapids, MI, USA, 25-30 June 2023 CY - Grand Rapids, MI, USA T2 - International Conference on RF Superconductivity T3 - 21 LA - english AB - We carried out in-situ NAXPS (Near-atmospheric X-ray Photoelectron Spectroscopy) on SRF-cavity class niobium to observe its oxidizing responses when exposed to various gases. The niobium samples were baked at 800°C until the peaks of niobium oxides disappeared in the spectrum. Then the revealed pure niobium samples were exposed to the air-proportion mixture of nitrogen and oxygen, pure oxygen, and pure water vapor respectively. And for the pure oxygen and water vapor group, we also carried out TOF-SIMS (Time-of-Flight Secondary Ion Mass Spectroscopy) measurements before and after the baking and oxidation experiments. We found that pure oxygen and water vapor could oxidize niobium at similar rate which was faster than the N2/O2 mixture. After re-oxidized by pure oxygen and water vapor, the niobium sample presented a significant increase of interstitial carbon and a moderate increase of interstitial oxygen in the magnetic penetration depth, while it showed a mild decrease of interstitial hydrogen. PB - JACoW Publishing CP - Geneva, Switzerland SP - 662 EP - 666 KW - niobium KW - cavity KW - experiment KW - SRF KW - vacuum DA - 2023/09 PY - 2023 SN - 2673-5504 SN - 978-3-95450-234-9 DO - doi:10.18429/JACoW-SRF2023-WEPWB045 UR - https://jacow.org/srf2023/papers/wepwb045.pdf ER -